I need to find: $A=\{x \in \mathbb{R}\vert\,\lfloor {2x} \rfloor + \lceil {x} \rceil - 4x = 0\}$
Let $x \in \mathbb{R}$. Then $$\begin{align*} \lceil {x} \rceil =4x- \lfloor {2x} \rfloor &\iff 4x- \lfloor {2x} \rfloor -1 < x \leq 4x -\lfloor {2x} \rfloor\\ &\iff \bigg[ 4x- \lfloor {2x} \rfloor -1 < x \bigg] \land \bigg[ x \leq 4x -\lfloor {2x} \rfloor \bigg]\\ &\iff (3x-1 < \lfloor {2x} \rfloor ) \land (\lfloor {2x} \rfloor \leq 3x) \end{align*} $$ Now define $B=\{x\in \mathbb R\mid(3x-1<\lfloor {2x} \rfloor \}$ and $C=\{x\in\mathbb R\mid\lfloor {2x} \rfloor \leq 3x\}$. Then $A=B\cap C$.
My confusion: $-\dfrac{2}{3} \in (B \cap C)$ but $-\dfrac{2}{3} \notin A$
In which step have I gone wrong?
The first step missed the condition that $\lceil x\rceil$ is an integer
The first step in your equivalence transformation as quoted below is wrong.
The definition of $\lceil x \rceil$ is "the least integer that is not smaller than $x$". Or, what is equivalent, "the integer that is $\ge x$ and $<x+1$". Hence, the first transformation should have been
$$ \lceil x\rceil =4x- \lfloor 2x\rfloor \\ \iff 4x- \lfloor 2x\rfloor \text{ is an integer and } x\le 4x- \lfloor 2x\rfloor < x +1 $$
A full solution
$\lceil x\rceil =4x- \lfloor 2x\rfloor$ implies $4x$ is an integer. There are three cases.
Then $x = 4x-2x$.
$x=0$
Then $\lceil x\rceil = x+\frac12$.
$x +\frac12 = 4x-2x$.
$x=\frac12$.
$x+\frac34=4x-(2x-\frac12)$
$x=\frac14$
$x+\frac14=4x-(2x-\frac12)$
$x=-\frac14$
Hence $x\in\{-\frac14, 0, \frac14, \frac12\}$.